EVA-DLLME-SFO聯合HPLC技術高通量檢測糕點中常見的添加劑

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High-Throughput Detection of Common Additives in Pastries by EVA-DLLME-SFO Combined with HPLC Technology

WANG Ying12， YAO Chenghu3， XIE Jun12， ZHAO Dandan'， HUANG Wei'

（1.College ofFoodEngineering，Ma’anshan Teacher’s College，Ma'anshan ，China; 2.InstituteofFood

and Health，Ma'anshan Teacher's Colege，Ma'anshan ， China; 3.Ma'anshan Institute of Product Quality Supervision and Inspection，Ma'anshan 243ooo， China）

Abstract： Objective： To establish an analytical method for the simultaneous determination of the contents of fouradditives in pastries byevaporation-asisted dispersive liquid-liquid microextraction based on the solidification of floating organic droplets （EVA-DLLME-SFO） coupled with high performance liquid chromatography （HPLC）. Method： Pastry samples were extracted using methanol aqueous solution （70：30，V/V） ， then extracted by EVA-DLLME-SFO method，determined by high performance liquid chromatography，and quantified by external standard method. Result： The linear relationship of the four additives was good within the range of 0.25μg?mL-1 to 50.00μg?mL-1 .The detection limit of the method was 1.8mg?kg-1 to 6.0mg?kg-1 ，the quantification limit was 6.0mg.kg-1 to 20.0mg?kg-1 ， the sample recovery rate was 88.54% to 98.85% ，and the relative standard deviation was （20 0.22% to 1.37% . Conclusion： This method is environmentally friendly and highly precise，and is suitable for the rapid detection of various additives in pastries.

Keywords： pastries; microextraction; liquid chromatography; additive; high throughput

為實現食品防腐或改善其色、香、味，根據《食品安全國家標準食品添加劑使用標準》（GB2760—2024），可在食品中添加天然或人工合成的食品添加劑。（剩余3301字）